Synthesis of Metal Oxide Nanoparticles in Flame Sprays: Review on Process Technology, Modeling, and Diagnostics

F. Meierhofer, U. Fritsching

Energy Fuels 35(7) 5495–5537 (2021)

DOI: 10.1021/acs.energyfuels.0c04054

Thermometry by Vibrational Raman Spectroscopy of Nitrogen: Identification and Impact of Spatial Averaging Effects

J. Kiefer, M.F.B. Stodt, U. Fritsching

J. Raman Spectrosc. 52(9) 1582–1588 (2021)

DOI: 10.1002/jrs.6104

Theoretical Investigation of Global Rainbow Refractometry in Spray Combustion of Polydisperse Microdroplets

M.F.B. Stodt, T. Wriedt, J. Kiefer, U. Fritsching

J. Mod. Opt. 68(5) (2021)

DOI: 10.1080/09500340.2021.1890251

Drop Dynamics in Heterogeneous Spray Flames for Nanoparticle Synthesis

M.F.B. Stodt, J. Kiefer, U. Fritsching

Atomization Sprays. 30(11) (2020)

DOI: 10.1615/AtomizSpr.2020034819

Quantification and Mitigation of PIV Bias Errors Caused by Intermittent Particle Seeding and Particle Lag by Means of Large Eddy Simulations

F. J. W. A. Martins, J. Kirchmann, A. Kronenburg, F. Beyrau

Measurement Science and Technology 32, 104006 (2021)

DOI: 10.1088/1361-6501/ac07d9

Single-Shot Two-Dimensional Multi-Angle Light Scattering (2D-MALS) Technique for Nanoparticle Aggregate Sizing

Martins, F. J. W. A., Kronenburg, A. and Beyrau, F.

Applied Physics B, 127 (51), (2021)

DOI: 10.1007/s00340-021-07599-5

Thermophysical Properties of Mixtures of Titanium(IV) Isopropoxide (TTIP) and 2-Propanol (iPOH)

A. Keller, I. Wlokas, M. Kohns, H. Hasse

Journal of Chemical & Engineering Data 66, 1296–1304 (2021)

DOI: 10.1021/acs.jced.0c00941

Solid-liquid Equilibria in Mixtures of Iron(III) Nitrate Nonahydrate and Ethanol or 1-Propanol

A. Keller, I. Wlokas, M. Kohns, H. Hasse

Fluid Phase Equilibria, 536 (15), 112987 (2021)

DOI: 10.1016/j.fluid.2021.112987

Tomographic imaging unig multi-simultaneous measurements (TIMes) for flame emission reconstructions

C. T. Foo, A. Unterberger, J. Menser and K. Mohri

Optics Express 29 (1), 224-255 (2021)

DOI: 10.1364/OE.412048

Two-phase sparse-Lagrangian MMC-LES of dilute ethanol spray flames

J. Kirchmann, A. Kronenburg, O. Stein, and M. Cleary

Proceedings of the Combustion Institute (2021) accepted for presentation

Influence of the dispersion gas flow on the spray-flame synthesis of LaMO3 (M = Mn, Fe, Co) functional perovskite nanomaterials

S. Angel, F. Schneider, W. Kaziur-Cegla, T. Schmidt, C. Schulz, H. Wiggers

Proceedings of the Combustion Institute (2021) accepted for presentation

Spray-flame synthesis of LaMO3 (M = Mn, Fe, Co) perovskite nanomaterials: effect of spray droplet size and esterification on particle size distribution

S. Angel, F. Schneider, W. Kaziur-Cegla, T. Schmidt, C. Schulz, H. Wiggers

Proceedings of the Combustion Institute (2021) accepted for presentation

Experimental and numerical investigation of iron-doped flames: FeO formation and impact on flame temperature

M. Nanjaiah, A.Pilipodi-Best, M. Lalanne, P. Fjodorow, C. Schulz, S. Cheskis, A. Kempf, I. Wlokas, I. Rahinov

Proceedings of the Combustion Institute (2021) accepted for presentation

Reference data set for three-dimensional measurements of double droplet combustion of p-xylene

H. Li, N. Riefler, T. Wriedt, L. Mädler

Proceedings of the Combustion Institute (2021) accepted for presentation

Laser Diagnostics of Flame Spray Pyrolysis for Iron Oxide Nanoparticle Synthesis

Stodt, M.F.B., Liu, C., Li, S., Mädler, L., Fritsching, U. Kiefer, J.

Proceedings of the Combustion Institute (2021) accepted for presentation

Insights into the Mechanism of Combustion Synthesis of Iron Oxide Nanoparticles Gained by Laser Diagnostics, Mass Spectrometry, and Numerical Simulations: A Mini-Review

I. Rahinov, J. Sellmann, M. R. Lallane, M. Nanjaiah, T. Dreie, S. Cheski, I. Wlokas

Energy Fuels 35 (1), 137–160 (2021)

DOI: 10.1021/acs.energyfuels.0c03561

Decomposition Reactions of Fe(CO)5, Fe(C5H5)2, and TTIP as Precursors for the Spray-Flame Synthesis of Nanoparticles in Partial Spray Evaporation at Low Temperatures

Munko Gonchikzhapov, Tina Kasper

Industrial & Engineering Chemistry Research 59 (18), 8551–8561 (2020)

DOI: 10.1021/acs.iecr.9b06667

Thermophysical Properties of Solutions of Iron(III) Nitrate-Nonahydrate in Mixtures of Ethanol and Water

A. Keller, I. Wlokas, M. Kohns, H. Hasse

Journal of Chemical & Engineering Data 65, 3519-3527 (2020)

DOI: 10.1021/acs.jced.0c00105

Thermophysical Properties of Solutions of Iron(III) Nitrate-Nonahydrate in Mixtures of 1-Propanol and Water

A. Keller, I. Wlokas, M. Kohns, H. Hasse

Journal of Chemical & Engineering Data 65, 5413-5420 (2020)

DOI: 10.1021/acs.jced.0c00531

Mathematical modeling of flash boiling phenomena in superheated sprays at low degree of superheat using Dirichlet hyperboloids

Bathia, B., De, A., and Gutheil, E.

Int. J. Multiphase Flow 130:130336 (2020)

DOI: 10.1016/j.ijmultiphaseflow.2020.103366

Thermophysical Properties of Mixtures of Titanium(IV) Isopropoxide (TTIP) and p-Xylene

A. Keller, I. Wlokas, M. Kohns, H. Hasse

Journal of Chemical & Engineering Data 65, 869-876 (2020)

DOI: 10.1021/acs.jced.9b01059

Large eddy simulation of a partially pre-vaporized ethanol reacting spray using the multiphase DTF/flamelet model

Hu, Y., Kai, R., Kurose, R., Gutheil, E., Olguin

International Journal of Multiphase Flow 125, 103216 (2020)

DOI: 10.1016/j.ijmultiphaseflow.2020.103216

Modeling and simulation of single ethanol/water droplet evaporation in dry and humid air

Narasu, P., Boschmann, S., Pöschko, P., Zhao, F., Gutheil, E.

Combustion Science and Technology, 192 (7), 1233-1252 (2020)

DOI: 10.1080/00102202.2020.1724980

The gas-phase formation of tin dioxide nanoparticles in single droplet combustion and flame spray pyrolysis

Li, H., Pokhrel, S., Schowalter, M., Rosenauer, A., Kiefer, J., Mädler, A.

Combust. Flame, 215, 389-400 (2020)

DOI: 10.1016/j.combustflame.2020.02.004

Nanoparticle evolution in flame spray pyrolysis–process design via experimental and computational analysis

F. Meierhofer, L. Mädler, U. Fritsching

AIChE J., 66 (2), e16885 (2020)

Nanoparticle formation and behavior in turbulent spray flames investigated by DNS

Abdelsamie, A., Kruis, E., Wiggers, H., Thévenin, D.

Flow, Turbulence and Combustion 105, 497–516 (2020)

DOI: 10.1007/s10494-020-00144-y

Gas-phase synthesis of iron oxide nanoparticles for improved magnetic hyperthermia performance

Hammad, M., Hardt, S., Mues, B., Salamon, S., Landers, J., Slabu, I., Wende, H., Schulz, C., Wiggers, H.

J. Alloys Compounds, 824, 153814 (2020)

DOI: 10.1016/j.jallcom.2020.153814

Spray-flame synthesis of BaTi1-xZrxO3 nanoparticles for energy storage applications

Tarasov, A., Shvartsman, V. V., Shoja, S., Lewin, D., Lupascu, D. C., Wiggers, H.

Ceramics International, 46 (9), 13915-13924 (2020)

DOI: 10.1016/j.ceramint.2020.02.187

Characterization of tracers for two-color laser-induced fluorescence liquid phase temperature imaging in sprays

M. Prenting, I. Bin Dzulfida, T. Dreier, C. Schulz

Exp. Fluids 61, 77 (2020)

DOI: 10.1007/s00348-020-2909-9

Experimental Investigation of Axisymmetric, Turbulent, Annular Jets Discharged Through the Nozzle of the SPP1980 SpraySyn Burner Under Isothermal and Reacting Conditions

F. J. W. A. Martins, J. Kirchmann, A. Kronenburg, F. Beyrau

Exp. Therm. FluidSci 114, 110052 (2020)

DOI: 10.1016/j.expthermflusci.2020.110052

Systematic assessment of the method of moments with interpolative closure and guidelines for its application to soot particle dynamics in laminar turbulent flames

A. Wick, M. Frenklach, H. Pitsch

Combustion and Flame, 214, 450-463 (2020)

DOI: 10.1016/j.combustflame.2020.01.007

Sparse-Lagrangian PDF modelling of silica synthesis from silane jets in vitiated co-flows with varying inflow conditions

G. Neuber, A. Kronenburg, O. Stein, C. E. Garcia, B. A. O. Williams, F. Beyrau, and M. J. Cleary

Flow, Turbulence and Combustion (2020)

DOI: 10.1007/s10494-020-00140-2

Closure of the scalar dissipation rate in the spray flamelet equations through a transport equation for the gradient of the mixture fraction

Olguin, H., Scholtissek, A., Gonzalez, S., Gonzalez, F., Ihme, M., Hasse, C., Gutheil, E.

Combustion and Flame 208, 330-350 (2019)

DOI: 10.1016/j.combustflame.2019.05.033

Ethanol Droplet Formation, Dynamics and Combustion Mode in the Flame of the SpraySynnozzle

Stodt, M.F.B., Kiefer, J., Fritsching, U

Exp. Fluids, 60, 125 (2019)

DOI: 10.1007/s00348-019-2771-9

Revealing the impact of laser-induced breakdown on a gas flow

Vanselow, C., Stöbener, D., Kiefer, J., Fischer, A.

Meas. Sci. Techn., 31, 027001(2019)

DOI: 10.1088/1361-6501/ab471e

Single droplet combustion of precursor/solvent solutions for nanoparticle production: Optical diagnostics on single isolated burning droplets with micro-explosions

H. Li, C.D. Rosebrock, Y. Wu, T. Wriedt, L. Mädler

Proc. Combust. Inst., 37, 1203-1211 (2019)

DOI: 10.1016/j.proci.2018.06.133

Experimental investigations on the effects of water vapor and oxygen concentrations in the ambience on the burning constant, lifetime and residuals of single isolated xylene, isobutanol and ethanol droplets

H. Li, C.D. Rosebrock, N. Riefler, T. Wriedt, L. Mädler

Exp. Thermal Fluid Sci. 109, 109920 (2019)

DOI: 10.1016/j.expthermflusci.2019.109920

Change of evaporation rate of single monocomponent droplet with temperature using time-resolved phase rainbow refractometry

Y. Wu, H. Li, X. Wu, G. Gréhan, L. Mädler, C. Crua

Proc. Combust. Inst. 37, 3211-3218 (2019)

DOI: 10.1016/j.proci.2018.09.026

Chemistry of iron nitrate-based precursor solutions for spray-flame synthesis

M.F.B. Stodt, M. Gonchikzhapov, T. Kasper, U. Fritsching, J. Kiefer

Physical Chemistry Chemical Physics 21, 24793–24801 (2019)

DOI: 10.1039/C9CP05007H

Gas-phase synthesis of functional nanomaterials: Challenges to kinetics diagnostics, and process development

C. Schulz, T. Dreier, M. Fikri, H. Wiggers

Proceedings of the Combustion Institute 37, 83-108 (2019)

DOI: 10.1016/j.proci.2018.06.231

SpraySyn - A standardized burner configuration for nanoparticle synthesis in spray flames

F. Schneider, S. Suleiman, J. Menser, E. Borukhovich, I. Wlokas, A. Kempf, H. Wiggers, C. Schulz

Rev. Sci. Instrum. 90, 085108 (2019)

DOI: 10.1063/1.5090232

Monte Carlo simulations of homogeneous nucleation and particle growth in the presence of background particles

Kotalczyk, G.; Skenderović, I.; Kruis, F.E.

Tellus B: Chemical and Physical Meteorology 71 (1), 1-10 (2019)

DOI: 10.1080/16000889.2018.1554415

On the behavior of spray combustion in a turbulent spatially-evolving jet investigated by direct numerical simulation

Abdelsamie, A. & Thévenin, D.

Proceeding of the Combustion Institute 37, 3373-3382, (2019)

DOI: 10.1016/j.proci.2018.06.016

Sparse-Lagrangian MMC modelling of the Sandia DME flame series

G.Neuber, F. Fuest, J. Kirchmann, A. Kronenburg, O. T. Stein, S. Galindo, M. J. Cleary, R. S. Barlow, B.Coriton, J. H. Frank, J. Sutton

Combust. Flame, 208:110-121 (2019)

DOI: 10.1016/j.combustflame.2019.06.026

Synthesis of silicon nanoparticles in a pilot-plant scale microwave plasma reactor: Impact of flow rates and precursor concentration on the nanoparticle size and aggregation

F. Kunze, S. Kuns, M. Spree, T. Hülser, C. Schulz, H. Wiggers, S. M.

Powder Technol. 342, 880-886 (2019)

DOI: 10.1016/j.powtec.2018.10.042

Unsupervised screening of vibrational spectra by principal component analysis for identifying molecular clusters

Kiefer, J., Eisen, K.

ChemPhysChem, 19, 795-800 (2018)

DOI: 10.1002/cphc.201701353

Fabrication and performance of Li4Ti5O12/C Li-ion battery electrodes using combined double flame spray pyrolysis and pressure-based lamination technique

M. Gockeln, S. Pokhrel, F. Meierhofer, J. Glenneberg, M. Schowalter, A. Rosenauer, U. Fritsching, M. Busse, L. Mädler, R. Kun

J. Power Sources, 374, 97-106 (2018)

DOI: 10.1016/j.jpowsour.2017.11.016

Dual Population Balance Monte Carlo Simulation of Particle Synthesis by Flame Spray Pyrolysis

Skenderović, I.; Kotalczyk, G.; Kruis, F.E.

Processes 6, 253 (2018)

DOI: 10.3390/pr6120253

Screening Precursor-Solvent Combinations for Li4Ti5O12 Energy Storage Material Using Flame Spray Pyrolysis

F. Meierhofer, H. Li, M. Gockeln, R. Kun, T. Grieb, A. Rosenauer, U. Fritsching, J. Kiefer, L. Mädler, S. Pokhrel

ACS Appl. Mat. Interf., 9 (43), 37760-37777 (2017)

Modification of a SAXS cameranto study structures on multiple scales

Gutsche, Alexander; Meier, Manuel; Guo, Xiaoai; Ungerer, Julian; Nirschl, Hermann

J Nanopart Res 19 (9), 1 (2017)

DOI: 10.1007/s11051-017-4017-1

SPP1980 Logo

CENIDE Logo

gefördert durch:
Dfg-logo

Prof. Dr. Christof Schulz
Universität Duisburg-Essen         
Fakultät für Ingenieurwissenschaften
Tel.: +49 203 379-8161
E-Mail: christof.schulz@uni-due.de